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Weak beam under convergent beam illumination

Schaublin1, Meng, Stobbs

  • 1Department of Materials Science and Metallurgy, University of Cambridge, UK. robin.schaeublin@psi.ch

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Summary

Accurately measuring dissociated dislocation spacing using the weak beam technique requires accounting for beam convergence. This study shows beam convergence is key for precise stacking fault energy determination in materials science.

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Area of Science:

  • Materials Science
  • Physical Metallurgy
  • Transmission Electron Microscopy

Background:

  • The weak beam technique is crucial for determining stacking fault energies, especially in intermetallic alloys.
  • Accurate measurement of dissociated dislocation spacing is vital for the reliability of this technique.
  • The relationship between dislocation image position and actual position is critical for accurate analysis.

Purpose of the Study:

  • To investigate the accuracy of determining partial dislocation spacing from weak beam images.
  • To explore the influence of various parameters on measurement accuracy, including beam convergence.
  • To model a dissociated dislocation in copper under specific weak beam conditions.

Main Methods:

  • Utilized image simulations for a model case of a dislocation dissociated into two Shockley partial dislocations in copper.
  • Examined orientations under the g(3g) weak beam condition at 100 kV.
  • Analyzed the impact of dislocation character, foil thickness, depth, diffraction condition, and beam convergence on measurement accuracy.

Main Results:

  • Image simulations indicate that a beam convergence of approximately 5 mrad significantly enhances measurement accuracy.
  • Beam convergence was identified as the principal parameter controlling the precision of partial dislocation spacing measurements.
  • The accuracy of determining true partial dislocation spacing is dependent on several factors, including beam convergence.

Conclusions:

  • Quantitative consideration of beam convergence is essential for accurately deducing true partial dislocation spacing.
  • Optimizing beam convergence improves the reliability of weak beam technique applications in materials characterization.
  • This study highlights the importance of precise simulation parameters for accurate dislocation analysis.