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2-Hydroxy-5-

Basu Baul TS¹, Dhar, Tiekink

¹Chemical Laboratory, Regional Sophisticated Instrumentation Centre, North Eastern Hill University, Bijni Complex, Shillong 793 003, India.

Acta Crystallographica. Section C, Crystal Structure Communications

|October 12, 2000

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This study details the crystal structure of a C(14)H(12)N(2)O(4) compound, revealing an E conformation and layered molecular arrangement. Carboxylic acid dimers primarily connect these layers, without significant pi-pi stacking interactions.

Area of Science:

Crystallography
Organic Chemistry
Materials Science

Background:

Understanding molecular conformation and intermolecular interactions is crucial for predicting material properties.
The specific compound C(14)H(12)N(2)O(4) has potential applications in [mention potential applications if known, otherwise omit].

Purpose of the Study:

To elucidate the crystal structure of the title compound, C(14)H(12)N(2)O(4).
To determine the conformation around the diazenyl nitrogen atoms.
To investigate the intermolecular interactions and packing motifs within the crystal lattice.

Main Methods:

Single-crystal X-ray diffraction was employed to determine the three-dimensional molecular structure.
Analysis of the crystal packing revealed the nature of intermolecular forces, including hydrogen bonding and van der Waals interactions.

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Main Results:

The title compound, C(14)H(12)N(2)O(4), adopts an E conformation about the diazenyl N-N bond.
The crystal structure is characterized by layered arrangements of molecules.
Carboxylic acid dimer motifs serve as the primary connecting units between adjacent molecular layers.
No significant evidence of extensive pi-pi stacking interactions between the layers was observed.

Conclusions:

The crystal structure of C(14)H(12)N(2)O(4) is primarily dictated by carboxylic acid dimer formation, leading to a layered architecture.
The absence of extensive pi-pi stacking suggests that other intermolecular forces dominate the crystal packing.
This structural information provides a foundation for understanding the compound's physical and chemical properties.