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Related Experiment Videos

Bismuth(V) iron(III) tris(phosphate) oxide.

A Benabad1, K Bakhous, F Cherkaoui

  • 1Laboratoire de Chimie du Solide Appliquée, Laboratoire Associé Francophone n501, Département de Chimie, Faculté des Sciences, Université Mohammed V-Agdal, Avenue Ibn Batouta, Rabat, Morocco.

Acta Crystallographica. Section C, Crystal Structure Communications
|November 15, 2000
PubMed
Summary
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This study details the crystal structure of Bismuth(V) Iron(III) Phosphate, revealing unique iron coordination and bismuth interstitial sites. The findings offer insights into complex inorganic material structures.

Area of Science:

  • Inorganic Chemistry
  • Crystallography
  • Materials Science

Background:

  • Understanding the atomic arrangement in complex inorganic compounds is crucial for materials science.
  • Bismuth and iron phosphates are of interest due to their diverse structural possibilities.

Purpose of the Study:

  • To elucidate the crystal structure of Bismuth(V) Iron(III) Phosphate (Bi(V)(0.4)Fe(3)(III)O(PO(4))(3)).
  • To characterize the coordination environments and atomic positions of bismuth and iron within the crystal lattice.

Main Methods:

  • Single-crystal X-ray diffraction was employed to determine the crystal structure.
  • Analysis of atomic positions, coordination numbers, and bond distances.

Main Results:

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  • The compound crystallizes with distinct iron coordination geometries: octahedral and trigonal bipyramidal.
  • Iron atoms form oxygen-bridged chains within the structure.
  • Bismuth(V) atoms occupy interstitial sites, exhibiting sevenfold coordination with Bi-O distances ranging from 2.357 to 2.529 Å.

    • Conclusions:

    • The crystal structure of Bi(V)(0.4)Fe(3)(III)O(PO(4))(3) has been successfully determined.
    • The study highlights the complex coordination chemistry of iron and bismuth in this phosphate material.