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4-Methyl-N-

Banerjee¹, Mukherjee, Nandi

¹Department of Physics, Jadavpur University, Calcutta 700 032, India.

Acta Crystallographica. Section C, Crystal Structure Communications

|December 19, 2000

Summary

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A novel palladium-copper-catalyzed reaction synthesized a unique organic compound. This molecule features three planar groups with specific dihedral angles and forms one-dimensional chains via hydrogen bonds.

Area of Science:

Organic Chemistry
Crystallography
Catalysis

Background:

Sulfonamides are versatile organic compounds with diverse applications.
Palladium-copper catalysis offers efficient synthetic routes for complex molecules.

Purpose of the Study:

To synthesize and characterize a novel organic compound.
To investigate the structural and bonding properties of the synthesized molecule.

Main Methods:

Palladium-copper-catalyzed cross-coupling reaction.
Single-crystal X-ray diffraction analysis.
Spectroscopic characterization (implied).

Main Results:

Successful synthesis of the title compound, C(20)H(19)NO(2)S(2).

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The molecule exhibits three approximately orthogonal planar moieties: aminothiophenol, toluenesulfone, and tolyl groups.

Defined dihedral angles (A/B: 111.6°, A/C: 89.3°, B/C: 101.4°) characterize the molecular conformation.

Intermolecular N-H···O hydrogen bonds result in infinite one-dimensional chains.

Conclusions:

The study reports a new synthetic methodology for a specific class of organic compounds.
The detailed structural analysis reveals unique molecular architecture and intermolecular interactions.
The formation of 1D chains highlights potential for supramolecular chemistry applications.