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Related Experiment Videos

1-Nitroindoline.

J Zaleski1, Z Daszkiewicz, J B Kyzioł

  • 1Institute of Chemistry, University of Opole, Oleska 48, 45-052 Opole, Poland. zaleski@uni.opole.pl

Acta Crystallographica. Section C, Crystal Structure Communications
|March 16, 2001
PubMed
Summary
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Acta crystallographica. Section C, Crystal structure communications·2001

This study details the crystal structure of a novel nitramine compound, C(8)H(8)N(2)O(2). Researchers found unique bonding characteristics and molecular arrangements, including planar nitramino groups and hydrogen-bonded chains.

Area of Science:

  • Organic Chemistry
  • Crystallography
  • Molecular Structure

Background:

  • Nitramine compounds are important in various chemical applications.
  • Understanding the molecular structure of novel compounds is crucial for predicting their properties.

Purpose of the Study:

  • To elucidate the detailed crystal structure of the compound C(8)H(8)N(2)O(2).
  • To analyze the bonding characteristics and intermolecular interactions within the crystal lattice.

Main Methods:

  • Single-crystal X-ray diffraction was employed to determine the molecular and crystal structure.
  • Analysis of bond lengths, bond angles, and intermolecular forces (hydrogen bonding) was performed.

Main Results:

  • The nitramino group was observed to be planar with slight twisting relative to the indoline rings.

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  • A shorter-than-typical bridgehead N--C bond and partial double-bond character in the N--N bond were identified.
  • Weak C--H...O hydrogen bonds were found to link molecules into chains along the z-axis.

    • Conclusions:

    • The study provides a comprehensive structural analysis of C(8)H(8)N(2)O(2).
    • The observed structural features, including bonding and hydrogen bonding, offer insights into the compound's chemical behavior and potential applications.