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Characterization of the solid state: quantitative issues.

G A Stephenson¹, R A Forbes, S M Reutzel-Edens

¹Lilly Research Laboratories, Eli Lilly and Company, Lilly Corporate Center, Indianapolis, IN 46285, USA. gas@lilly.com

Advanced Drug Delivery Reviews

|April 28, 2001

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Accurate quantitative phase analysis is crucial for drug safety and pharmaceutical manufacturing. This article reviews common techniques and essential considerations for developing precise solid-state methods.

Area of Science:

Pharmaceutical Sciences
Materials Science
Analytical Chemistry

Background:

Quantitative analysis of solid-state composition is vital for drug safety and pharmaceutical production control.
Various techniques exist for quantifying phase composition, each with unique challenges.

Purpose of the Study:

To describe common techniques for quantitative phase analysis.
To outline considerations for developing accurate and precise solid-state methods.

Main Methods:

Review of established quantitative phase analysis techniques.
Discussion of method development considerations for solid-state characterization.

Main Results:

Identification of multiple common techniques for quantitative phase analysis.

Related Experiment Videos

Highlighting accuracy and precision challenges in solid-state method development.

Conclusions:

Selecting the appropriate quantitative phase analysis technique is critical.
Careful consideration of method development factors ensures reliable solid-state composition analysis.