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Monitoring solid-phase glycoside synthesis with (19)F NMR spectroscopy
M Mogemark1, M Elofsson, J Kihlberg
1Organic Chemistry, Department of Chemistry, Umeå University, SE-901 87 Umeå, Sweden.
Organic Letters
|June 5, 2001
Abstract:
[structure: see text] A simple and efficient method for monitoring and optimizing carbohydrate synthesis on polymeric support by using (19)F NMR spectroscopy is described. The method relies on the use of fluorinated variants of protective groups that are in common use in oligosaccharide synthesis.