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N-(2-hydroxyethyl)ethylenediammonium hydrogenphosphate monohydrate.

Selcuk Demir1, Veysel T Yilmaz, Omer Andac

  • 1Department of Chemistry, Faculty of Arts and Science, Ondokuz Mayis University, 55139 Kurupelit Samsun, Turkey.

Acta Crystallographica. Section C, Crystal Structure Communications
|July 3, 2002
PubMed
Summary

This study reveals a novel crystal structure with alternating layers of hydrogenphosphate and N-(2-hydroxyethyl)ethylenediammonium. Hydrogen bonds and water molecules within voids stabilize this unique layered material.

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Area of Science:

  • Crystal chemistry
  • Materials science
  • Supramolecular chemistry

Background:

  • Layered materials offer unique properties for various applications.
  • Understanding the role of hydrogen bonding and guest molecules is crucial for crystal engineering.

Purpose of the Study:

  • To elucidate the crystal structure of the title compound, C(4)H(14)N(2)O(2+) x HPO(4)(2-) x H(2)O.
  • To investigate the arrangement of inorganic and organic components within the crystal lattice.
  • To analyze the role of water molecules and hydrogen bonding in stabilizing the structure.

Main Methods:

  • Single-crystal X-ray diffraction was employed to determine the three-dimensional crystal structure.
  • Analysis of intermolecular interactions, including hydrogen bonds, was performed.

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Main Results:

  • The crystal structure exhibits alternating, interleaved layers of hydrogenphosphate anions and N-(2-hydroxyethyl)ethylenediammonium cations.
  • Water molecules are located within channel-like voids, participating in the hydrogen bonding network.
  • A robust network of hydrogen bonds plays a key role in stabilizing the overall crystal packing.

Conclusions:

  • The title compound represents a novel layered material with potential applications in areas requiring specific host-guest interactions.
  • The intricate hydrogen bonding network and the presence of water molecules are critical for the structural integrity and stability of this material.