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Updated: Sep 29, 2026

Determination of Inorganic Arsenic in a Wide Range of Food Matrices using Hydride Generation - Atomic Absorption Spectrometry.
Published on: September 1, 2017
Reagent injection FIA system for lead determination by hydride generation - quartz-tube atomic absorption
M T Baranguan1, F Laborda, J R Castillo
1Analytical Spectroscopy and Sensors Group, Department of Analytical Chemistry, University of Zaragoza, Spain.
Abstract:
A method is proposed for the determination of lead by generation of its hydride and detection by quartz-tube AAS using a reagent injection FIA system based on the injection of sodium tetrahydroborate. Lead hydride generation was carried out using a combination of 0.5 M nitric acid, 10% m/ v hydrogen peroxide and 10% m/ v sodium tetrahydroborate. The characteristic concentration obtained was 3.1 ng mL(-1) and the detection limit was 2.6 ng mL(-1) for an injected volume of 0.125 mL of tetrahydroborate.
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