Jove
Visualize
Contact Us
JoVE
x logofacebook logolinkedin logoyoutube logo
ABOUT JoVE
OverviewLeadershipBlogJoVE Help Center
AUTHORS
Publishing ProcessEditorial BoardScope & PoliciesPeer ReviewFAQSubmit
LIBRARIANS
TestimonialsSubscriptionsAccessResourcesLibrary Advisory BoardFAQ
RESEARCH
JoVE JournalMethods CollectionsJoVE Encyclopedia of ExperimentsArchive
EDUCATION
JoVE CoreJoVE BusinessJoVE Science EducationJoVE Lab ManualFaculty Resource CenterFaculty Site
Terms & Conditions of Use
Privacy Policy
Policies

Related Experiment Videos

Solid-state NMR spectroscopic methods in chemistry.

David D Laws1, Hans-Marcus L Bitter, Alexej Jerschow

  • 1Materials Sciences Division, Lawrence Berkeley National Laboratory and Department of Chemistry, University of California at Berkeley, Berkeley, CA 94720, USA.

Angewandte Chemie (International Ed. in English)
|September 11, 2002
PubMed
Summary
This summary is machine-generated.

Related Concept Videos

You might also read

Related Articles

Articles linked to this work by shared authors, journal, and citation graph.

Sort by
Same author

Revealing Hidden Dynamics of Hydrogel-Based Desalination with <sup>23</sup>Na Nuclear Magnetic Resonance.

The journal of physical chemistry. C, Nanomaterials and interfaces·2026
Same author

Lithium Nuclear Spin Polarization Lifetimes as Sensitive Reporters of Battery Electrolyte Degradation.

ACS omega·2026
Same author

Over four minutes of pyruvate T<sub>1</sub> using chemically and physically induced deceleration of relaxation.

Nature communications·2026
Same author

Enabling nondestructive observation of electrolyte composition in batteries with ultralow-field nuclear magnetic resonance.

Chemical science·2026
Same author

Identifying intermolecular multiple-quantum coherences in ionic liquids.

Journal of magnetic resonance (San Diego, Calif. : 1997)·2025
Same author

Molecular Shells and Range of Interactions in Ionic Liquids as a Function of Temperature.

The journal of physical chemistry letters·2025

Solid-state NMR spectroscopy is a powerful technique for analyzing solid materials, offering high resolution and unique insights. Advances in methods like magic-angle spinning enhance its capabilities for chemical analysis and structure determination.

Area of Science:

  • Analytical Chemistry
  • Spectroscopy
  • Materials Science

Background:

  • Nuclear Magnetic Resonance (NMR) spectroscopy is vital for chemical analysis and structure determination across various scientific disciplines.
  • While typically used for liquid samples, solid-state NMR is increasingly important for studying solid materials.
  • This review focuses on the advancements and applications of solid-state NMR spectroscopy.

Purpose of the Study:

  • To review key developments in solid-state NMR spectroscopy techniques.
  • To highlight the applications of these techniques in structure determination.
  • To discuss the growing importance and future potential of solid-state NMR.

Main Methods:

  • Cross-polarization
  • Magic-angle spinning (MAS)

Related Experiment Videos

  • Multiple-pulse sequences
  • Homo- and heteronuclear decoupling and recoupling
  • Multiple-quantum spectroscopy
  • Dynamic angle spinning (DAS)

    • Main Results:

    • Modern solid-state NMR achieves resolution comparable to liquid-state NMR.
    • These techniques leverage anisotropic interactions, providing information often inaccessible in liquid samples.
    • Solid-state NMR enables detailed structural analysis of solid samples and materials.

    Conclusions:

    • Solid-state NMR spectroscopy has evolved into a powerful analytical tool.
    • Its advanced techniques offer high resolution and unique insights into molecular structures.
    • The field shows significant promise for future applications in chemistry and materials science.