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[Sensitive and rapid analysis of nitrophenols and herbicides by capillary zone electrophoresis (CZE)]
1Dalian Institute of Chemical Physics, Chinese Academy of Sciences, 116012 Dalian, China.
Se Pu = Chinese Journal of Chromatography
|January 25, 2003
Abstract:
11 Nitrophenols and some acidic herbicides have been separated by modified CZE. Good separation of such compounds can be achieved in less than 10 min by simply modifying the run buffer with organic solvents such as methanol, acetonitrile in a concentration of 40% (V/V). The limits of detection (LODs) for nitrophenols by UV-absorption at 215 nm were 0.5 mg/L-1.1 mg/L. Solid phase extraction was used to preconcentrate nitrophenols and some herbicides to reach an LOD at microgram/L levels. Typical samples have been analyzed.