Related Experiment Video
Updated: Sep 27, 2026

Standardized Protocol to Evaluate the Effect of Surface Treatments, Luting Cements, and Thermocycling on PEEK–Composite Bond Strength
Published on: June 9, 2026
Polymerization contraction stress in dual-cure cements and its effect on interfacial integrity of bonded inlays
Roberto R Braga1, Jack L Ferracane, John R Condon
1Department of Dental Materials, School of Dentistry, University of São Paulo, Av Prof Lineu Prestes, 2227, São Paulo, SP 00508-900, Brazil. rrbraga@usp.br
Objectives:
To compare the polymerization contraction stress of resin cements in dual-cure and self-cure modes, and verify its effect on microleakage and gap formation in class I cavities restored with porcelain inlays.
Methods:
Dual-cure cements (Calibra, Choice and RelyX ARC) were monitored for contraction stress during 30 min in the tensilometer, in the presence or absence of photo-activation. Microleakage was evaluated in porcelain inlays bonded to cavities prepared in bovine incisors, combining the same adhesive (One-Step) with each of the cements in both activation modes. Epoxy replicas of the sectioned specimens were analyzed in the SEM to determine the percentage of discontinuous margins.
Results:
The stress developed in dual-cure mode was higher than in self-cure mode for all cements. In self-cure mode, no significant difference in stress was found among materials. Choice and RelyX ARC showed higher microleakage in dual-cure mode than in self-cure mode. Calibra did not show a significant difference in microleakage between activation modes. Contraction gap results showed wide variations, and no significant differences were detected among the groups. Gaps occurred more often in dentin, with an overall average of 22 +/- 17.5%.
Conclusions:
The higher stress generated in dual-cure cements subjected to photo-activation may lead to higher marginal leakage. In the confinement condition represented by the class I inlay, even the lower contraction stress of the cements in self-cure mode had enough magnitude to disrupt the bonding to dentin.
Related Concept Videos
Bonding and Strength of Aggregate
Microcracking in Concrete
Curing of Concrete
Strength of Cement
For compressive strength tests, ASTM C 109-05 standards prescribe a cement-sand mix ratio of 1:2.75 and a water/cement ratio of 0.485 for making 2-inch cubes. These cubes are mixed, cast, and cured in saturated lime water at 23°C until testing. Flexural strength testing, outlined in ASTM C...
Hydration of Cement
Creep in Concrete
