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Novel one-pot vicinal double C-acylation of styrenes and methacrylates by electroreduction
Yoshimasa Yamamoto1, Hirofumi Maekawa, Satoshi Goda
1Department of Chemistry, Nagaoka University of Technology, 1603-1, Kamitomioka-cho, Nagaoka, Niigata 940-2188, Japan.
Organic Letters
|July 19, 2003
Abstract:
[reaction: see text] Electroreduction of styrenes or alkyl methacrylates in the presence of aliphatic acid anhydrides or N-acylimidazoles with an undivided cell equipped with zinc electrodes as the anode and the cathode brought about novel one-pot vicinal double C-acylation to afford the corresponding 1,4-diketones in satisfactory yields.