Jove
Visualize
Contact Us
JoVE
x logofacebook logolinkedin logoyoutube logo
ABOUT JoVE
OverviewLeadershipBlogJoVE Help Center
AUTHORS
Publishing ProcessEditorial BoardScope & PoliciesPeer ReviewFAQSubmit
LIBRARIANS
TestimonialsSubscriptionsAccessResourcesLibrary Advisory BoardFAQ
RESEARCH
JoVE JournalMethods CollectionsJoVE Encyclopedia of ExperimentsArchive
EDUCATION
JoVE CoreJoVE BusinessJoVE Science EducationJoVE Lab ManualFaculty Resource CenterFaculty Site
Terms & Conditions of Use
Privacy Policy
Policies

Related Experiment Videos

Solid-phase microextraction for herbicide determination in environmental samples.

L J Krutz1, S A Senseman, A S Sciumbato

  • 1Department of Soil & Crop Sciences, Texas Agricultural Experiment Station, Texas A&M University, College Station, TX 77843-2474, USA. lkrutz@ag.tamu.edu

Journal of Chromatography. A
|July 30, 2003
PubMed
Summary

Solid-phase microextraction (SPME) offers a faster, solventless alternative for determining herbicide residues in environmental samples. This review covers SPME theory, methods, and applications for enhanced environmental analysis.

Related Concept Videos

You might also read

Related Articles

Articles linked to this work by shared authors, journal, and citation graph.

Sort by
Same author

Transitioning from conventional to cover crop systems with minimum tillage does not alter nutrient loading.

Journal of environmental quality·2022
Same author

Stability of Selected Pesticides on Solid-Phase Extraction Disks.

Journal of environmental quality·2021
Same author

Influence of Soil Moisture Zones on Rice Water Weevil (Coleoptera: Curculionidae) Populations in Furrow Irrigated Rice.

Environmental entomology·2021
Same author

Evaluation of Flood Removal in Combination with Insecticide Seed Treatment for Rice Water Weevil (Coleoptera: Curculionidae) Larval Management in Rice.

Journal of economic entomology·2020
Same author

Application of Polyacrylamide (PAM) through Lay-Flat Polyethylene Tubing: Effects on Infiltration, Erosion, N and P Transport, and Corn Yield.

Journal of environmental quality·2017
Same author

Susceptibility of Flowering Cotton to Damage and Yield Loss from Tarnished Plant Bug (Hemiptera: Miridae).

Journal of economic entomology·2016

Area of Science:

  • Environmental Chemistry
  • Analytical Chemistry

Background:

  • Traditional methods for herbicide residue determination in environmental samples include liquid-liquid extraction or solid-phase extraction coupled with gas chromatography (GC) or high-performance liquid chromatography.
  • These conventional techniques often involve significant solvent use and can be time-consuming.

Purpose of the Study:

  • To review the existing literature on Solid-Phase Microextraction (SPME) for herbicide residue analysis.
  • To explore SPME's extraction theory, various extraction modes, and suitable fiber types.
  • To discuss method optimization and current/future applications of SPME in environmental matrices.

Main Methods:

  • Literature review of scientific publications on SPME for herbicide determination.
  • Analysis of extraction principles, operational parameters, and fiber technologies relevant to SPME.

Related Experiment Videos

  • Synthesis of information on the application of SPME across different environmental sample types.

    • Main Results:

    • Solid-phase microextraction (SPME) is presented as a solventless, rapid, and sensitive extraction technique.
    • SPME demonstrates versatility for application across diverse environmental matrices.
    • The review consolidates knowledge on SPME optimization for effective herbicide residue analysis.

    Conclusions:

    • SPME is a viable and advantageous alternative to traditional extraction methods for environmental herbicide residue analysis.
    • Further research and optimization can expand the scope and efficiency of SPME applications.
    • SPME facilitates improved environmental monitoring and risk assessment through sensitive and sustainable residue determination.