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Separation, recovery and recycling of a fluorous-tagged nickel catalyst using fluorous solid-phase extraction
Ben Croxtall1, Eric G Hope, Alison M Stuart
1Department of Chemistry, University of Leicester, Leicester, UK LE1 7RH.
Abstract:
Highly efficient separation, recovery and recycling of the fluorous-tagged catalyst, [Ni[F13C6C(O)CHC(O)C6F13]2], can be achieved with fluorous solid-phase extraction, after the Lewis acid catalysed synthesis of enaminodiones in conventional organic solvents.