Jove
Visualize
Contact Us
JoVE
x logofacebook logolinkedin logoyoutube logo
ABOUT JoVE
OverviewLeadershipBlogJoVE Help Center
AUTHORS
Publishing ProcessEditorial BoardScope & PoliciesPeer ReviewFAQSubmit
LIBRARIANS
TestimonialsSubscriptionsAccessResourcesLibrary Advisory BoardFAQ
RESEARCH
JoVE JournalMethods CollectionsJoVE Encyclopedia of ExperimentsArchive
EDUCATION
JoVE CoreJoVE BusinessJoVE Science EducationJoVE Lab ManualFaculty Resource CenterFaculty Site
Terms & Conditions of Use
Privacy Policy
Policies

Related Experiment Videos

Microstructural and microtextural characterization of oxide scale on steel using electron backscatter diffraction.

S Birosca1, D Dingley, R L Higginson

  • 1IPTME: Institute of Polymer Technology and Materials Engineering, Loughborough University, Loughborough, Leicestershire LE11 3TU, UK.

Journal of Microscopy
|March 11, 2004
PubMed
Summary

Investigating iron oxide scales on steel using electron back-scatter diffraction (EBSD) reveals critical microstructural details. This research enhances understanding of oxide behavior during steel processing and removal.

Related Concept Videos

You might also read

Related Articles

Articles linked to this work by shared authors, journal, and citation graph.

Sort by
Same author

Using wire shaping techniques and holographic optics to optimize deposition characteristics in wire-based laser cladding.

Proceedings. Mathematical, physical, and engineering sciences·2017
Same author

Nanostructure characterisation of flow-formed Cr-Mo-V steel using transmission Kikuchi diffraction technique.

Ultramicroscopy·2015
Same author

Interface study by dual-beam FIB-TEM in a pressureless infiltrated Al(Mg)-Al2O3 interpenetrating composite.

Journal of microscopy·2009
Same author

Texture evolution in grain-oriented electrical steel during hot band annealing and cold rolling.

Journal of microscopy·2008
Same author

Oxide formation and alloying elements enrichment on TRIP steel surface during inter-critical annealing.

Journal of microscopy·2008
Same author

Phase determination and microstructure of oxide scales formed on steel at high temperature.

Journal of microscopy·2005

Area of Science:

  • Materials Science
  • Metallurgy
  • Surface Engineering

Background:

  • High-temperature oxidation of steel is a significant industrial concern.
  • Understanding iron oxide scale microstructure is crucial for steel processing and post-processing.
  • Conventional microscopy methods struggle to resolve oxide microstructures effectively.

Purpose of the Study:

  • To investigate the microstructure and microtexture of iron oxide layers formed on interstitial free steel.
  • To evaluate the effectiveness of electron back-scatter diffraction (EBSD) in characterizing these oxide scales.
  • To correlate oxide characteristics with varying oxidation times and temperatures under industrial conditions.

Main Methods:

  • Utilized electron back-scatter diffraction (EBSD) for detailed microstructural and microtextural analysis.

Related Experiment Videos

  • Performed heat treatments under normal oxidation conditions simulating industrial steel manufacturing.
  • Analyzed oxide composition, morphology, microstructure, and microtexture using EBSD.

    • Main Results:

    • EBSD successfully distinguished different phases within the iron oxide scales.
    • Valuable information on microstructure and orientation relationships between steel and scale layers was obtained.
    • Microstructure and microtexture of oxide layers were characterized at different times and temperatures.

    Conclusions:

    • Electron back-scatter diffraction (EBSD) is a powerful technique for analyzing iron oxide scales on steel.
    • The study provides critical insights into oxide scale behavior relevant to steel manufacturing processes.
    • Understanding oxide microstructure and texture aids in optimizing steel processing and scale removal strategies.