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High-performance flow atomic spectrometry: New nebulization techniques, on-line speciation and on-line sample
1Institut für Spektrochemie und angewandte Spektroskopie, Bunsen-Kirchhoffstrasse 11, D-44139, Dortmund, Germany.
Analytical and Bioanalytical Chemistry
|June 1, 1996
Abstract:
An interface-free combination of HPLC separation techniques and methods for element determination by atomic spectrometry can be achieved by hydraulic high-pressure nebulization (HHPN). With high-temperature HHPN (300 ( degrees )C) super heated liquids can be nebulized providing aerosol yields of up to 90% in flame AAS. This new nebulization method combines the advantages of HHPN and thermospray techniques (very small aerosol droplets, high aerosol yield, nebulization of saturated salt solutions).