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Updated: Aug 25, 2026

Methods of Ex Situ and In Situ Investigations of Structural Transformations: The Case of Crystallization of Metallic Glasses
Published on: June 7, 2018
Mössbauer and X-ray studies of Fe-powder mechanically alloyed with C using power ultrasonics
V M Nadutov1, B N Mordyuk, G I Prokopenko
1G.V. Kurdyumov Institute for Metal Physics, National Academy of Science of Ukraine, 36 Acad. Vernadsky Blvd. 03680 Kyiv 142, Ukraine. nadvl@imp.kiev.ua
Abstract:
The Mössbauer and X-rays analysis of as-received Fe-powder and Fe-powder mechanically alloyed with C using high power ultrasonics were carried out. The powder blend of Fe-powder and graphite was processed in He environment during 5 to 50 h. The dissolution of carbon in iron particles and inhomogeneous distribution of C atoms in crystallites was revealed. The ultrasonic milling of the f.c.c. Fe-Ni-powder with graphite was carried out. As established, the saturation of iron particles with carbon under ultrasonic milling occurs for much shorter time as compared to the high-energy ball milling.

