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Updated: Aug 23, 2026
A Direct, Early Stage Guanidinylation Protocol for the Synthesis of Complex Aminoguanidine-containing Natural Products
Published on: September 9, 2016
Studies towards the total synthesis of batzelladine A
Mark C Elliott1, Matthew S Long
1School of Chemistry, Cardiff University, PO Box 912, Cardiff, UKCF10 3TB. elliottmc@cardiff.ac.uk
Abstract:
Application of a diastereoselective three-component coupling to the bicyclic core of the batzelladine alkaloids is described. The synthesis features the elaboration of glutamic acid by use of Eschenmoser sulfide contraction. An earlier approach is also included, which shows some limitations of dithiane chemistry when applied to the particular compounds required for this target.
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