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Related Experiment Videos

Bis(triethanolamine-O,O')nickel(II) diacetate.

Ingmar Krabbes1, Wilhelm Seichter, Karsten Gloe

  • 1Institut für Anorganische Chemie, TU Dresden, D-01062 Dresden, Germany.

Acta Crystallographica. Section C, Crystal Structure Communications
|July 21, 2004
PubMed
Summary

A novel nickel compound, [Ni{N(CH(2)CH(2)OH)(3)}(2)](CH(3)COO)(2), was synthesized and its structure elucidated. This new compound is isostructural with its copper(II) counterpart, indicating similar coordination chemistry.

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Supramolecular Motifs in the Crystal Structures of Triethylbenzene Derivatives Bearing Pyridinium Subunits in Combination with Pyrimidinyl or Pyridinyl Groups.

Molecules (Basel, Switzerland)·2023

Area of Science:

  • Coordination chemistry
  • Inorganic chemistry
  • Materials science

Background:

  • Nickel complexes are vital in catalysis and materials science.
  • Understanding the structural properties of metal complexes informs their function.
  • Isostructural compounds provide insights into electronic and steric effects.

Purpose of the Study:

  • To synthesize and characterize a new nickel coordination compound.
  • To determine the crystal structure of the title compound.
  • To compare its structure with related metal analogues.

Main Methods:

  • Chemical synthesis of the nickel complex.
  • Single-crystal X-ray diffraction for structural determination.
  • Comparison with crystallographic data of the copper(II) analogue.

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Main Results:

  • Successful synthesis of the title nickel compound, [Ni{N(CH(2)CH(2)OH)(3)}(2)](CH(3)COO)(2).
  • The crystal structure was determined, revealing its coordination environment.
  • The compound was found to be isostructural with the corresponding copper(II) complex.

Conclusions:

  • The synthesis and structural determination of the nickel compound were achieved.
  • The isostructural relationship highlights similarities in coordination preferences between nickel and copper(II) in this ligand system.
  • This finding contributes to the understanding of structure-property relationships in coordination complexes.