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Related Experiment Videos

N-Acetyl-L-phenylalanine.

K L Stout1, K J Hallock, J W Kampf

  • 1Biophysics Research Division, Room 3004, University of Michigan, Ann Arbor, MI 48109-1055, USA.

Acta Crystallographica. Section C, Crystal Structure Communications
|July 21, 2004
PubMed
Summary
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The crystal structure of C(11)H(13)NO(3) reveals a unique 2D network. This network is formed by intermolecular hydrogen bonds, specifically N-H.O and O-H.O interactions.

Area of Science:

  • Crystal engineering
  • Supramolecular chemistry
  • Materials science

Background:

  • Understanding intermolecular forces is crucial for designing novel materials.
  • Hydrogen bonding plays a pivotal role in the self-assembly of molecular structures.
  • The specific compound C(11)H(13)NO(3) was synthesized for structural investigation.

Purpose of the Study:

  • To elucidate the crystal structure of C(11)H(13)NO(3).
  • To characterize the hydrogen bonding network within the crystal lattice.
  • To provide insights into the supramolecular assembly of this compound.

Main Methods:

  • Single-crystal X-ray diffraction was employed to determine the atomic arrangement.
  • Analysis of intermolecular interactions, focusing on hydrogen bonds.

Related Experiment Videos

  • Structural data was interpreted to understand the network formation.

    • Main Results:

    • The compound C(11)H(13)NO(3) forms a two-dimensional infinite network in the solid state.
    • The network is stabilized by a combination of N-H.O and O-H.O intermolecular hydrogen bonds.
    • Detailed crystallographic analysis confirmed the specific geometry and connectivity of these hydrogen bonds.

    Conclusions:

    • The crystal structure of C(11)H(13)NO(3) is characterized by a robust 2D hydrogen-bonded network.
    • This supramolecular architecture arises from specific intermolecular N-H.O and O-H.O interactions.
    • The findings contribute to the understanding of crystal packing and hydrogen bonding in organic compounds.