Jove
Visualize
Contact Us
JoVE
x logofacebook logolinkedin logoyoutube logo
ABOUT JoVE
OverviewLeadershipBlogJoVE Help Center
AUTHORS
Publishing ProcessEditorial BoardScope & PoliciesPeer ReviewFAQSubmit
LIBRARIANS
TestimonialsSubscriptionsAccessResourcesLibrary Advisory BoardFAQ
RESEARCH
JoVE JournalMethods CollectionsJoVE Encyclopedia of ExperimentsArchive
EDUCATION
JoVE CoreJoVE BusinessJoVE Science EducationJoVE Lab ManualFaculty Resource CenterFaculty Site
Terms & Conditions of Use
Privacy Policy
Policies

Related Experiment Videos

Veneering composites - a thermoanalytical examination.

M Rosentritt1, M Behr, A Leibrock

  • 1Department of Prosthetic Dentistry, University of Regensburg, 93042 Regensburg, Germany.

Journal of Materials Science. Materials in Medicine
|September 7, 2004
PubMed
Summary

This study used thermal analysis to examine five dental veneering composites. Each material was tested after being cured for different times using manufacturer devices. The samples were immediately analyzed to avoid post-curing effects. Results showed distinct thermal events like glass transition and polymerization peaks. These thermal signatures varied across materials and curing times. The study suggests that thermal analysis can help classify composites based on their thermal behavior. This approach may improve material selection and quality control in dental applications.

Related Concept Videos

You might also read

Related Articles

Articles linked to this work by shared authors, journal, and citation graph.

Sort by
Same author

High rate of safety and fraud issues in commercially available cinnamon.

NPJ science of food·2025
Same author

Exploring the influence of parametrized pulsatility on left ventricular washout under LVAD support: a computational study using reduced-order models.

Computer methods in biomechanics and biomedical engineering·2025
Same author

In-silico analysis of hemodynamic indicators in idealized stented coronary arteries for varying stent indentation.

Computer methods in biomechanics and biomedical engineering·2024
Same author

Effect of apical root resection, orthodontic extrusion, and surgical crown lengthening on load capability.

Clinical oral investigations·2023
Same author

[Emergency overcrowding and hospital organization: Causes and solutions].

La Revue de medecine interne·2020
Same author

Exploratory study of the three-dimensional morphological variation of the jaw associated to teeth loss.

Journal of stomatology, oral and maxillofacial surgery·2019

Area of Science:

  • Dental materials science
  • Polymer chemistry
  • Thermal analysis in material science

Background:

Current research on dental composites often focuses on mechanical and optical properties. Less attention has been given to thermal behavior during curing. Prior studies show that composites undergo phase changes and polymerization that affect their final properties. However, the precise thermal signatures of veneering composites remain unclear. This gap motivated the use of thermal analysis to classify these materials. No prior work had resolved how thermal curing times influence composite structure. Existing methods do not fully capture post-polymerization effects. This paper introduces a new approach to analyze composites using thermal data. The study aims to provide a framework for identifying material characteristics through thermal profiles.

Purpose Of The Study:

The goal was to assess thermal behavior of veneering composites during curing. The specific problem is understanding how different composites respond to thermal treatment. The motivation comes from the need to classify materials based on thermal signatures. This study seeks to identify key thermal events like glass transition and polymerization. The authors aim to provide a classification system using thermal data. They also want to compare curing behaviors across different brands. The study focuses on how thermal profiles correlate with composite composition. This work may help in selecting materials based on their thermal response.

Keywords:
dental compositesthermal gravimetric analysispolymer curingmaterial classification

Frequently Asked Questions

Glass transition and polymerization peaks occurred between 30 and 100 degrees C, with post-polymerization peaks between 150 and 300 degrees C.

Samples were made from five composites and subjected to thermal curing times of 4 s to 25 min using manufacturer devices.

To prevent post-curing during storage, samples were subjected to a dynamic temperature program at 10 degrees C per minute.

Filler and matrix content differences were detectable through thermal profiles, aiding in material classification.

Related Experiment Videos

Main Methods:

The study used differential thermal analysis and thermal gravimetric analysis. Samples of five veneering composites were tested in 4-20 mg quantities. The materials included Visio-Gem, Sinfony, Artglass, Dentacolor, and Targis. Each sample underwent thermal curing for 4 s to 25 min using manufacturer devices. A control group of unreacted samples was also analyzed. To prevent post-curing, all samples were immediately subjected to a dynamic temperature program. The heating rate was set at 10 degrees C per minute. The thermal data captured events like glass transition and polymerization peaks.

Main Results:

The thermal profiles revealed distinct characteristics for each composite material. Glass transition and polymerization peaks occurred between 30 and 100 degrees C. Additional peaks were observed between 150 and 300 degrees C, indicating post-polymerization. The position of these peaks varied across the five materials tested. Filler and matrix content differences were detectable through thermal analysis. Curing time influenced the thermal behavior of each composite. The control group showed no polymerization peaks, confirming the method's accuracy. These findings suggest thermal analysis can classify veneering composites effectively.

Conclusions:

The authors propose that thermal analysis can distinguish veneering composites based on material characteristics. They suggest that thermal profiles reflect polymerization and post-polymerization events. The study indicates that thermal data may help in material classification. The authors propose that filler and matrix content can be inferred from thermal peaks. They suggest that curing time affects the thermal signature of each composite. The authors propose that this method may be useful in quality control settings. The study suggests that thermal analysis provides a non-destructive way to assess composites. The authors propose that this approach may improve the selection of dental materials.

Curing time influenced thermal signatures, with different composites showing varied responses to thermal treatment.

The authors propose that thermal analysis may improve material classification and selection in dental applications.