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Characterisation of (17)O-enriched alumina from a new hydrothermal preparation

Burkhard C Schmidt1, Fabrice Gaillard, Mark E Smith

  • 1Bayerisches Geoinstitut, Universität Bayreuth, D-95440 Bayreuth, Germany. burkhard.schmidt@uni-bayreuth.de

Solid State Nuclear Magnetic Resonance
|September 25, 2004
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In addition to the oxymercuration–demercuration method, which converts the alkenes to alcohols with Markovnikov orientation, a complementary hydroboration-oxidation method yields the anti-Markovnikov product. The hydroboration reaction, discovered in 1959 by H.C. Brown, involves the addition of a B–H bond of borane to an alkene giving an organoborane intermediate. The oxidation of this intermediate with basic hydrogen peroxide forms an alcohol.