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Electrospinning Fundamentals: Optimizing Solution and Apparatus Parameters
Published on: January 21, 2011
Nanofibers of LiMn2O4 by electrospinning
Na Yu1, Changlu Shao, Yichun Liu
1Center for Advanced Optoelectronic Functional Materials Research, Northeast Normal University, Changchun 130024, People's Republic of China.
Abstract:
Through sol-gel processing and electrospinning technique, extrathin fibers of poly(vinyl alcohol) (PVA)/lithium chloride/manganese acetate composite fibers were prepared. After calcination of the above precursor fibers at 600 degrees C, the spinel lithium manganese oxide (LiMn2O4) nanofibers, with a diameter of 100-200 nm, were successfully obtained. The fibers were investigated by TG-DTA, XRD, FT-IR, and SEM, respectively. The results showed that the crystalline phase and morphology of the fibers were largely influenced by the calcination temperature.

