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[Li(MoO2)2O(AsO4)].

Mounir Hajji1, Mohamed Faouzi Zid, Tahar Jouini

  • 1Laboratoire de Matériaux et Cristallochimie, Faculté des Sciences de Tunis, Université de Tunis ElManar, 2092 El Manar II Tunis, Tunisie.

Acta Crystallographica. Section C, Crystal Structure Communications
|May 7, 2005
PubMed
Summary
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Researchers synthesized single crystals of lithium bis(dioxomolybdenum) arsenate oxide, Li(MoO2)2O(AsO4), revealing a layered structure with corner-shared Mo2AsO12 units and square-pyramidal lithium environments.

Area of Science:

  • Solid-state chemistry
  • Inorganic materials science
  • Crystallography

Context:

  • Molybdenum arsenates are an emerging class of inorganic materials with potential applications in catalysis and energy storage.
  • Understanding the structural intricacies of these compounds is crucial for tailoring their properties.
  • Previous studies have explored various molybdenum-based oxides and arsenates, but the specific layered structure of Li(MoO2)2O(AsO4) warrants detailed investigation.

Purpose:

  • To synthesize single crystals of Li(MoO2)2O(AsO4) using solid-state reaction methods.
  • To elucidate the crystal structure of Li(MoO2)2O(AsO4), focusing on the arrangement of Mo2AsO12 units and Li+ ion coordination.
  • To compare the structural features of Li(MoO2)2O(AsO4) with related compounds containing M2O9 dimers.

Summary:

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  • Single crystals of lithium bis(dioxomolybdenum) arsenate oxide, Li(MoO2)2O(AsO4), were successfully prepared via solid-state reaction.
  • The crystal structure is characterized by layered arrangements of corner-shared Mo2AsO12 units, formed from AsO4 tetrahedra and Mo2O9 dimers.
  • Lithium ions occupy inter-layer sites within a square-based-pyramidal coordination environment.

Impact:

  • The detailed structural characterization provides fundamental insights into the bonding and architecture of molybdenum arsenate compounds.
  • The findings contribute to the broader understanding of layered inorganic materials and their potential for novel applications.
  • Comparison with related M2O9 dimer-containing structures highlights structure-property relationships in this material class.