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Resonant soft X-ray diffraction - in extremis.

P D Hatton1, S B Wilkins, T A W Beale

  • 1Department of Physics, University of Durham, Rochester Building, South Road, Durham DH1 3LE, UK. p.d.hatton@dur.ac.uk

Journal of Synchrotron Radiation
|June 22, 2005
PubMed
Summary
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This study explores using low-energy X-rays for diffraction, detailing experiments with resonant scattering. This technique aids in observing subtle effects like magnetic and orbital ordering in materials.

Area of Science:

  • Materials Science
  • Condensed Matter Physics
  • X-ray Crystallography

Background:

  • Soft X-ray diffraction is gaining interest for materials analysis.
  • Resonant scattering at L absorption edges of 3d transition metals is a key area.

Purpose of the Study:

  • To report experiments using soft X-rays for diffraction.
  • To highlight advantages for studying weak diffraction effects.

Main Methods:

  • Utilizing synchrotron radiation for soft X-ray generation.
  • Conducting experiments at L absorption edges (500-1000 eV).
  • Employing a windowless high-vacuum vessel due to severe absorption.

Main Results:

  • Demonstrated resonant scattering at L absorption edges.

Related Experiment Videos

  • Addressed challenges of high absorption and small Ewald sphere.
  • Showcased utility for weak diffraction phenomena.

    • Conclusions:

    • Soft X-ray diffraction at L edges is feasible despite technical challenges.
    • This method offers unique insights into anomalous scattering, charge, magnetic, and orbital ordering.