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Updated: Aug 16, 2026

Rapid Collection of Floral Fragrance Volatiles using a Headspace Volatile Collection Technique for GC-MS Thermal Desorption Sampling
Published on: December 10, 2019
[Analysis of volatile components from the flowers of Chrysanthemum morifolium by GC-MS with solid-phase
Hai-mei Zhou1, Pei-shan Xie, Wan-hui Wang
1Henan University of Science and Technology, Luoyang 471003, China. lyzhm@xin-huanet.com
Objective:
To study a method for extraction and analysis of volatile components from Chrysanthemum morifolium 'gonghuangjv' cv. nov (CM GHJ) and C. morifolium 'gongbaijv' cv. nov (CM GBJ) by solid-phase microextraction (SPME) and gas chromatography-mass spectrometry (GC-MS).
Method:
The volatile components were extracted in different temperature, different balance period and different extraction fiber using head space solid-phase microextraction (HS-SPME), and were identified by CGC-MS. The variety in integral area of each component was observed in different conditions and its relative content was determined by normalization of area.
Result:
The better condition of SPME for C. morifolium was that the sample was extracted using 100 microm polydimethylsiloxane (PDMS) extraction fiber after it had been balanced for 6 hours at 75 degrees C. 53 components from CM GHJ and CM GBJ were identified, and there were 35 same components in CM GHJ and CM GBJ.
Conclusion:
HS-SPME-GC-MS is convenient, rapid and reliable for analysis of volatile components in C. morifolium.
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