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Published on: November 23, 2016
A model study toward the total synthesis of N-deacetyllappaconitine
Douglass F Taber1, Jiang-Lin Liang, Bei Chen
1Department of Chemistry and Biochemistry, University of Delaware, Newark, 19716, USA. taberdj@udel.edu
The Journal of Organic Chemistry
|October 22, 2005
Abstract:
[reaction: see text] A model study leading to the preparation of the AEF rings of N-deacetyllappaconitine is described. The conjugate addition to the alpha-alkyl cyclohexenone 10 proceeded with high diastereocontrol. The Mannich cyclization of 16 to 4 was accomplished by heating with Rexyn-300 and Na(2)SO(4).
