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[Determination of acetochlor and oxyfluorfen by capillary gas chromatography]
Wen-Sheng Xiang1, Xiang-Jing Wang, Jing Wang
1Center of Life Science, Northeast Agricultural University, Harbin 150030, China. xiangwensheng@yahoo.com.cn
Abstract:
A method is described for the determination of acetochlor and oxyfluorfen by capillary gas chromatography with FID and an SE-30 capillary column (60 m x 0.53 mm i. d., 1.5 microm), using dibutyl phthalate as the internal standard. The standard deviations for acetochlor and oxyfluorfen concentration(mass fraction) were 0.44% and 0.47% respectively. The relative standard deviations for acetochlor and oxyfluorfen were 0.79% and 0.88% and the average recoveries for acetochlor and oxyfluorfen were 99.3% and 101.1% respectively. The method is simple, rapid and accurate.
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