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Effect of grinding and heating on Ni2+ uptake properties of waste paper sludge

Vinay Kumar Jha1, Yoshikazu Kameshima, Akira Nakajima

  • 1Department of Metallurgy and Ceramics Science, Tokyo Institute of Technology, O-okayama, Meguro, Tokyo, Japan.

Journal of Environmental Management
|March 25, 2006
PubMed

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Precipitation Gravimetry

Precipitation gravimetry is based on converting an analyte into a sparingly soluble precipitate, which is separated by filtration and weighed. An ideal precipitate should be pure, insoluble, of known composition, and easily filtered from the reaction mixture.
In determining nickel by gravimetric analysis, a precipitant of ethanolic dimethylglyoxime is added to a hot nickel salt solution. This is quickly followed by the dropwise addition of dilute ammonia solution until precipitation occurs. A...