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Updated: Aug 8, 2026

Online Size-exclusion and Ion-exchange Chromatography on a SAXS Beamline
Published on: January 5, 2017
High-throughput asymmetric double-crystal monochromator of the SAXS beamline at ELETTRA
S Bernstorff1, H Amenitsch, P Laggner
1Sincrotrone Trieste, Strada Statale per Basovizza 14 km 163.5, 34012 Trieste, Italy.
Abstract:
A new high-flux wiggler beamline for fast time-resolved small-angle X-ray scattering (SAXS) based on double-focusing optics has recently commenced operation at the 2 GeV third-generation storage ring ELETTRA at Trieste, Italy. Its non-dispersive double-crystal monochromator contains three pairs of interchangeable asymmetrically cut flat Si(111)-crystal pairs, each of which is optimized for high throughput at one of the three fixed energies 5.4, 8 and 16 keV. To cope with the severe thermal power load produced by a 57-pole wiggler on the first crystal of each pair (up to 5.4 W mm(-2) and 700 W under normal incidence, for 400 mA), grazing angles of 2 degrees and optimized back-cooling have been chosen. This solution allows simultaneously a gain of 2.5-3.0 in throughput and, accordingly, in flux density. Finite-element analysis as well as commissioning tests showed that the cooling layout functions very satisfactorily, and that up to 5 x 10(12) photons s(-1) are available at the sample (at 8 keV and 250 mA), as predicted.

