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Updated: Aug 7, 2026

Fabrication, Densification, and Replica Molding of 3D Carbon Nanotube Microstructures
Published on: July 2, 2012
Tubular carbon nano-/microstructures synthesized from graphite powders by an in situ template process
Guozhen Shen1, Yoshio Bando, Chunyi Zhi
1Advanced Materials Laboratory, National Institute for Materials Science, Namiki 1-1, Tsukuba, Ibaraki 304-0044, Japan. Shen.Guozhen@nims.go.jp
Abstract:
Through the use of commercial graphite powders as the carbon sources, a variety of interesting tubular carbon nano- and microstructures, such as networked carbon nanotubes, aligned carbon microtubes with hexagonal cross-sections, aligned tapered carbon tubes, and hollow carbon microhorns, have been successfully synthesized. As-grown tubular carbon structures were characterized using scanning electron microscopy, transmission electron microscopy, and X-ray energy-dispersive spectroscopy. An in situ template mechanism was proposed to explain the possible growth process. The vibrational properties of the synthesized tubular carbon structures were also studied by Raman spectroscopy.

