Related Experiment Video
Updated: Jul 19, 2026

In Situ Characterization of Boehmite Particles in Water Using Liquid SEM
Published on: September 27, 2017
Charging compensation of alumina samples by using an oxygen microinjector in the environmental scanning electron
Xueling Quan1, Yuan Ji, Hong Zhang
1Institute of Microstructure and Property of Advanced Materials, Beijing University of Technology, Beijing, China.
Abstract:
A gas microinjector system was set up in an environmental scanning electron microscope (ESEM) to create an oxygen atmosphere around the alumina samples for the charging compensation under a pressure between 2 x 10(-5) Pa approximately 2 x 10(-2) Pa. At low pressures, the skirt effect of the electron scattering can be degraded, which results in improvement of the imaging contrast and increase of the signal/noise ratio. The sample current (I(SC)) and the Duane-Hunt limit were measured to evaluate the charging effect.
More Related Videos
08:31Probing Surface Electrochemical Activity of Nanomaterials using a Hybrid Atomic Force Microscope-Scanning Electrochemical Microscope (AFM-SECM)
Published on: February 10, 2021
08:00A Synthetic Methodology for Preparing Impregnated and Grafted Amine-Based Silica Composites for Carbon Capture
Published on: September 29, 2023
Related Concept Videos
Preparation of Samples for Electron Microscopy
Scanning Electron Microscopy
Fundamental Principles
Accelerated...