Related Experiment Video
Updated: Jul 18, 2026
Thin Film Composite Silicon Elastomers for Cell Culture and Skin Applications: Manufacturing and Characterization
Published on: July 3, 2018
Effect of temperature on unpolymerized composite resin film thickness
John S Blalock1, Robert G Holmes, Frederick A Rueggeberg
1School of Dentistry, Medical College of Georgia, Augusta, GA 30912-1260, USA. jblalock@mail.mcg.edu <jblalock@mail.mcg.edu>
Statement Of Problem:
Room temperature (RT) composite resins are viscous, and this condition may affect the ability of the material to flow and adapt to preparation walls.
Purpose:
The purpose of this study was to compare the film thickness of a variety of commercial composite resins heated prior to light polymerization. The film thickness of these heated materials was also compared to those of flowable products at RT.
Material And Methods:
Five flowable and 7 conventional composite resins were used: 2 microfills, a nanofill hybrid, 2 submicron hybrids, a trimodal hybrid, and a packable. Composite resin (0.05 mL) was pressed between 2 Mylar-covered glass plates (15 kg) for 180 seconds, light polymerized, and the thickness measured using a micrometer. When comparing conventional composite resin heated to 54 degrees C or 60 degrees C, the RT value was control, while the RT flowable values were control when compared to heated composite resin. (n=5/group). Data were analyzed using 1- and 2-way analysis of variance and the Tukey-Kramer post hoc test (alpha=.05). Correlation of filler content to flow potential was evaluated. Scanning electron microscopic analysis of polymerized specimens was characterized by filler size and shape.
Results:
Room temperature conventional composite resin values varied in film thickness. Not all preheated products reduced in thickness. Thickness of the nanofill did not reduce, and one of the submicron hybrids reduced the greatest. No correlation existed between composite resin classification, filler content or shape, and film thickness. No difference in thickness existed between composite resins preheated to 54 degrees C and 60 degrees C. Room temperature and preheated conventional composite resin provided film thickness greater than that of flowable materials.
Conclusions:
Preheating conventional composite resin yields lower film thickness for some products, but flow cannot be attributed to composite resin classification, filler content, or shape. Preheated composite resin thickness was greater than that of all flowables.
Related Concept Videos
02:28Effect of Temperature Change on Reaction Rate
01:26Polymer Classification: Stereospecificity
01:14Polymer Classification: Architecture
01:21Polymer Classification: Crystallinity
Crystalline domains are the regions where polymer chains are aligned in an orderly manner and held together in proximity by intermolecular forces. For example, chains in the crystalline domains of polyethylene and nylon are bound together by van der Waals...
02:55Temperature Dependence on Reaction Rate
Atoms, molecules, or ions must collide before they can react with each other. Atoms must be close together to form chemical bonds. This premise is the basis for a theory that explains many observations regarding chemical kinetics, including factors affecting reaction rates.
The collision theory is based on the postulates that (i) the reaction rate is proportional to the rate of reactant collisions, (ii) the reacting species collide in an orientation allowing contact between...