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Reverse Microemulsion-mediated Synthesis of Monometallic and Bimetallic Early Transition Metal Carbide and Nitride Nanoparticles
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Ultra-rapid processing of refractory carbides; 20 s synthesis of molybdenum carbide, Mo2C

Simon R Vallance1, Sam Kingman, Duncan H Gregory

  • 1School of Chemistry, University Of Nottingham, University Park, Nottingham, UKNG7 2RD.

Chemical Communications (Cambridge, England)
|March 30, 2007
PubMed

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Alkenes via Reductive Coupling of Aldehydes or Ketones: McMurry Reaction01:22

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The radical dimerization of ketones or aldehydes gives vicinal diols through a pinacol coupling reaction. However, the behavior of titanium metals used for the reaction as a source of electrons is unusual. When the reaction is carried out in the presence of titanium, diols can be isolated at low temperatures. Else titanium further reacts with diols, forming alkenes through the McMurry reaction.