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Disposable sample holder for high temperature measurements in MPMS superconducting quantum interference device

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Researchers developed a low-cost aluminum foil sample holder for high-temperature measurements using superconducting quantum interference device magnetometers. This disposable holder minimizes background signals, ensuring accurate results for solid and powder samples.

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Area of Science:

  • Materials Science
  • Condensed Matter Physics
  • Quantum Technologies

Background:

  • Superconducting Quantum Interference Device (SQUID) magnetometers require precise sample manipulation for accurate measurements.
  • High-temperature measurements (300 K to 800 K) present challenges for sample holder design due to thermal expansion and material stability.
  • Minimizing background signals is crucial for detecting weak magnetic responses.

Purpose of the Study:

  • To present a novel, cost-effective sample holder for high-temperature SQUID magnetometry.
  • To demonstrate the suitability of the holder for both solid and powder samples.
  • To quantify the background signal contribution of the proposed sample holder.

Main Methods:

  • Fabrication of a sample holder using readily available aluminum foil.
  • Testing the holder's performance in a SQUID magnetometer across a temperature range of 300 K to 800 K.
  • Characterization of the holder's magnetic homogeneity and background signal contribution.

Main Results:

  • The aluminum foil sample holder is suitable for high-temperature (300 K < T < 800 K) SQUID measurements.
  • The holder exhibits excellent magnetic homogeneity, resulting in a background signal below the instrument noise level (<10(-9) A m2 at μ(0)H=200 mT).
  • The holder is inexpensive, simple to fabricate, and disposable, preventing cross-contamination.

Conclusions:

  • A practical and economical sample holder for high-temperature SQUID magnetometry has been developed.
  • The design effectively minimizes background noise, enhancing measurement sensitivity.
  • The disposable nature of the holder offers convenience and ensures sample integrity for future experiments.