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Framework materials assembled from magnesium carboxylate building units.

Robert P Davies1, Robert J Less, Paul D Lickiss

  • 1Department of Chemistry, Imperial College London, South Kensington, London, UKSW7 2AZ. r.davies@imperial.ac.uk

Dalton Transactions (Cambridge, England : 2003)
|June 15, 2007
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This study synthesized four magnesium-based coordination polymers using various dicarboxylic and tricarboxylic acids. These materials exhibit diverse structures, including 2D layers and 3D networks, with potential for solid-state interconversion.

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Area of Science:

  • Materials Science
  • Inorganic Chemistry
  • Crystallography

Background:

  • Coordination polymers offer tunable structures and properties.
  • Magnesium-based materials are of interest for various applications.
  • Carboxylic acids serve as versatile organic linkers in coordination chemistry.

Purpose of the Study:

  • To synthesize and structurally characterize novel magnesium-based coordination polymers.
  • To investigate the impact of different organic linkers on network topology.
  • To explore the solid-state reactivity and interconversion of these materials.

Main Methods:

  • Single crystal X-ray diffraction for structural determination.
  • Synthesis using magnesium nitrate and various carboxylic acids (H(2)bdc, H(2)bpdc, H(3)btc).
  • Powder X-ray diffraction and thermogravimetric analysis for solid-state studies.

Main Results:

  • Four coordination polymers with magnesium nodes and di-/tri-carboxylic acids were synthesized.
  • Structures ranged from 2D layered to 3D cubic networks, influenced by linker length and metal node aggregation.
  • Compounds 1 and 2 showed interconversion with simpler magnesium carboxylates and hydrates.

Conclusions:

  • The choice of organic linker significantly dictates the resulting coordination polymer architecture.
  • Magnesium coordination polymers can exhibit diverse structural motifs, including layered and 3D frameworks.
  • The synthesized materials demonstrate potential for solid-state transformations.