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Updated: Jul 8, 2026

Improving High Viscosity Extrusion of Microcrystals for Time-resolved Serial Femtosecond Crystallography at X-ray Lasers
Published on: February 28, 2019
Photometric measurement of linear crystallization velocity on a microscale
L J Soltzberg1, Y M Dick, J M Stowe
1Simmon College, Chemistry Department, Boston, Massachusetts 02115, USA.
Abstract:
Use of a photometer-equipped polarizing microscope permits the measurement of linear crystallization velocity in a flexible manner. Ease of sample preparation and manipulation compared with conventional methods for measuring crystallization velocity are among the advantages of the method reported here. A simple barrier layer silicon photodetector in short-circuit operation gives the fast response necessary to follow the moving solid-liquid interface. Sample results on the crystallization of alpha- and beta-resorcinol illustrate the utility of this method.
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