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An Efficient Method for the Synthesis of Peptoids with Mixed Lysine-type/Arginine-type Monomers and Evaluation of Their Anti-leishmanial Activity
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An efficient chemical-enzymatic synthesis of LHRH N-terminal pentapeptide

U Slomczynska1, T Leplawy, M T Leplawy

  • 1Institute of Organic Chemistry, Technical University, Lodz, Poland.

Biomedica Biochimica Acta
|January 11, 1991
PubMed

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Direct alkylation is not a suitable method for synthesizing amines because it produces polyalkylated products. Gabriel synthesis is the most preferred method to exclusively make primary amines. The method uses phthalimide, which contains a protected form of nitrogen that participates in alkylation only once to predominantly give primary amines.
Strong bases like NaOH or KOH deprotonate the phthalimide to form the corresponding anion, which acts as a nucleophile. Further, the anion attacks an...