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Updated: Jul 6, 2026

Preparation of Food Samples Using Homogenization and Microwave-Assisted Wet Acid Digestion for Multi-Element Determination with ICP-MS
Published on: December 22, 2023
[Determination of nutrition elements in Yak milk powder by atomic absorption spectrometry]
Yan Shi1, Wei-wan Zheng, Wei-wei Xiao
1Key Laboratory of Food Science of MOE, Nanchang 330047, China. kwei@ncu.edu.cn
Abstract:
In the present paper, orthogonal design test was planed by changing cinefaction temperature, cinefaction time, and the concentration of hydrochloric acid. Yak milk powder and milk powder were digested by dry method. The contents of elements Ca, Mg, Fe, Cu, Zn, Mn, K and Na were determined by flame atomic absorption spectrometry. The best conditions for the digestion were obtained as follows: the temperature was 510 degrees C, cinefaction time 4 hours, and hydrochloric acid concentration 1 : 5. Meanwhile, under the best experimental conditions, the recovery ratio of the method in the range of 95.2%-107.3%, and the relative standard deviations were 0.38%-3.86% (n=6). The experimental results proved that Yak milk powder is valuable and nutritious food, and has rich nutrition elements.
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