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Related Concept Videos

X-ray Crystallography02:18

X-ray Crystallography

The size of the unit cell and the arrangement of atoms in a crystal may be determined from measurements of the diffraction of X-rays by the crystal, termed X-ray crystallography.
Diffraction
Diffraction is the change in the direction of travel experienced by an electromagnetic wave when it encounters a physical barrier whose dimensions are comparable to those of the wavelength of the light. X-rays are electromagnetic radiation with wavelengths about as long as the distance between neighboring...
Determination of Crystal Structures01:29

Determination of Crystal Structures

In the late 1800s, the revelation that light extended beyond visible wavelengths led to the discovery of X-rays by Wilhelm Roentgen. Recognized as high-energy electromagnetic radiation with short wavelengths, X-rays prompted exploration into their interaction with crystals. Max von Laue proposed in 1912 that the periodic arrangement of atoms, ions, or molecules in crystals would cause them to diffract X-rays, a hypothesis confirmed through experiments with copper sulfate and zinc sulfide...
Unsymmetric Bending - Angle of Neutral Axis01:15

Unsymmetric Bending - Angle of Neutral Axis

Unsymmetrical bending occurs when a structural member is subjected to bending moments in a plane that does not align with the member's principal axes. This scenario typically arises in beams and other structural components when loads are applied at non-ideal angles, introducing complexities in stress analysis.
When a bending moment is applied at an angle θ concerning the vertical axis of a symmetrical member, it can be resolved into components along the member's principal centroidal axes. The...
Adjusting a Traverse01:12

Adjusting a Traverse

In the site survey of a four-sided traverse, internal angles are essential to ensure geometric accuracy. The survey revealed that the sum of the measured internal angles was 359 degrees and 48 minutes, which is 12 minutes less than the expected 360 degrees. This discrepancy signals an error likely arising from measurement inaccuracies during the fieldwork.To rectify this error, the adjustment process involved distributing the 12-minute shortfall equally across the four internal angles. By...

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Related Experiment Video

Updated: Jul 6, 2026

Microfluidic Chips for In Situ Crystal X-ray Diffraction and In Situ Dynamic Light Scattering for Serial Crystallography
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Microfluidic Chips for In Situ Crystal X-ray Diffraction and In Situ Dynamic Light Scattering for Serial Crystallography

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Accurate miscut angle determination for spherically bent Bragg crystals.

D S Covita1, M Ay, S Schlesser

  • 1Departamento de Física, Universidade de Coimbra, 3004-516 Coimbra, Portugal. daniel.covita@psi.ch

The Review of Scientific Instruments
|April 2, 2008
PubMed
Summary
This summary is machine-generated.

We present a straightforward method to measure the crystal cut angle and orientation for spherically bent crystals. This technique combines X-ray diffraction and laser alignment for precise analysis in spectroscopy applications.

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Area of Science:

  • Atomic and Molecular Physics
  • Materials Science
  • Spectroscopy

Background:

  • Spherically bent crystals are crucial for high-resolution spectroscopy, especially in low count-rate experiments like exotic-atom research.
  • Accurate focal conditions depend on bending radius, Bragg angle, crystal cut angle, and orientation relative to dispersion.

Purpose of the Study:

  • To develop and present a simple, precise method for measuring the cut angle and orientation of mounted spherically bent crystals.
  • To facilitate accurate setup and performance of crystal analyzers in spectroscopic applications.

Main Methods:

  • Combines X-ray diffraction and laser optical alignment.
  • Utilizes standard X-ray laboratory equipment for ease of implementation.

Main Results:

  • Successfully demonstrates a method for precise measurement of crystal cut angle and orientation.
  • Provides a practical approach for characterizing spherically bent crystal analyzers.

Conclusions:

  • The described method offers a simple yet accurate way to determine critical parameters of spherically bent crystals.
  • This technique is valuable for optimizing crystal analyzers in demanding spectroscopic research.