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Related Concept Videos

IR Spectrometers01:25

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There are two main infrared (IR) spectrophotometers: dispersive IR spectrometers and Fourier transform infrared (FTIR) spectrometers. In a dispersive IR spectrometer, a beam of infrared radiation produced by a hot wire is divided into two parallel equal-intensity beams using mirrors. One beam passes through the sample, while another is a reference beam. The beams then move through the monochromator, which separates the radiations into a continuous spectrum of different frequencies. The...
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Updated: Jul 2, 2026

A Stable Phantom Material for Optical and Acoustic Imaging
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Published on: June 16, 2023

X-ray reflectometer for optical efficiency and scatter measurements.

J M Reynolds1, S A Fields, R L Holland

  • 1Space Sciences Laboratory, NASA/Marshall Space Flight Center, AL 35812, USA.

The Review of Scientific Instruments
|December 1, 1978
PubMed
Summary

A new instrument measures x-ray reflection efficiency and scatter for optical samples. It achieves high resolution, enabling detailed characterization of materials like fused silica for advanced optics.

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Area of Science:

  • Optics and Materials Science
  • X-ray instrumentation and metrology

Background:

  • Accurate characterization of optical sample reflectivity and scatter is crucial for x-ray applications.
  • Existing methods may lack the precision required for advanced optical metrology at x-ray wavelengths.

Purpose of the Study:

  • To develop and validate a novel instrument for measuring x-ray reflection efficiency and scatter.
  • To characterize optical properties of fused silica samples using the developed reflectometer.

Main Methods:

  • An oil-free vacuum chamber reflectometer was designed to measure reflection efficiency and scatter.
  • Measurements were performed as a function of the angle of incidence for x-ray wavelengths (1.5–113 Å).
  • Instrument resolution was determined using least-squares smoothing of experimental data.

Main Results:

  • Reflection efficiency was measured for fused silica (flatness λ/10) at 8.34 Å and compared to theoretical data.
  • Scatter curves were obtained for direct and reflected x-ray beams.
  • The instrument demonstrated a full-width-at-half-maximum (FWHM) resolution of approximately 13 arc seconds.

Conclusions:

  • The developed instrument provides precise measurements of x-ray reflection efficiency and scatter.
  • The findings validate the instrument's capability for characterizing optical materials for x-ray applications.
  • High-resolution characterization is essential for the development of advanced x-ray optical components.