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Related Concept Videos

Inductively Coupled Plasma Atomic Emission Spectroscopy: Principle01:19

Inductively Coupled Plasma Atomic Emission Spectroscopy: Principle

Inductively coupled plasma (ICP) is the most widely used plasma source in atomic emission spectroscopy (AES), also known as Inductively Coupled Plasma Optical Emission Spectroscopy (ICP-OES). The ICP source, or torch, consists of three concentric quartz tubes with argon gas flowing through them. A spark from a Tesla coil initiates the ionization of argon, generating a high-temperature plasma.
The ions and electrons produced interact with the fluctuating magnetic field created by a water-cooled...
Inductively Coupled Plasma–Mass Spectrometry (ICP–MS): Overview01:19

Inductively Coupled Plasma–Mass Spectrometry (ICP–MS): Overview

In inductively coupled plasma–mass spectrometry (ICP–MS), an inductively coupled plasma (ICP) torch is used as an atomizer and ionizer. Solid samples are dissolved and volatilized before being introduced into the high-temperature argon plasma, while solution samples are nebulized and passed through the high-temperature argon plasma. Plasma dissociates the analytes and ionizes their component atoms to form a mixture of positive ions and molecular species. The positive ions are then passed on to...
Atomic Emission Spectroscopy: Overview01:20

Atomic Emission Spectroscopy: Overview

Atomic emission spectroscopy (AES) is an analytical technique used to determine the elemental composition of a sample by analyzing the light emitted from excited atoms. In AES, atoms in a sample are excited to higher energy levels by thermal energy from high-temperature sources, such as plasma, arcs, or sparks. When these excited atoms return to lower energy states, they emit light at specific wavelengths characteristic of each element. The resulting atomic emission spectrum, which consists of...
Standing Waves in a Cavity01:28

Standing Waves in a Cavity

A household microwave and lasers are examples of standing electromagnetic waves in a cavity. When two conducting metal plates are placed parallel at the nodal planes, it creates a cavity where standing waves are formed. The cavity between the two planes is analogous to a stretched string held at the points x = 0 and x = L. Here, the distance 'L' between the two planes must be an integer multiple of half of the wavelength. The wavelengths that satisfy this condition are given by:
Atomic Emission Spectroscopy: Instrumentation01:22

Atomic Emission Spectroscopy: Instrumentation

The instrumentation of atomic emission spectrometry (AES) involves various components, including atomization devices that convert samples into gas-phase atoms and ions. There are two main types of atomization devices: continuous and discrete atomizers.  Continuous atomizers, like plasmas and flames, introduce samples in a constant stream, while discrete atomizers inject individual samples using syringes or autosamplers. The most common discrete atomizer is the electrothermal atomizer.
Atomic Emission Spectroscopy: Lab01:29

Atomic Emission Spectroscopy: Lab

AES is a powerful analytical technique, especially effective when used with plasma sources, producing abundant spectra in characteristic emission lines. The Inductively Coupled Plasma (ICP), in particular, yields superior quantitative analytical data due to its high stability, low noise, low background, and minimal interferences under optimal experimental conditions. However, newer air-operated microwave sources are emerging as promising alternatives that could be more cost-effective than...

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Related Experiment Video

Updated: Jul 2, 2026

How to Ignite an Atmospheric Pressure Microwave Plasma Torch without Any Additional Igniters
08:42

How to Ignite an Atmospheric Pressure Microwave Plasma Torch without Any Additional Igniters

Published on: April 16, 2015

Simple automatic initiator for microwave induced plasmas.

H R Crowe1, I B Goldberg

  • 1Science Center, Rockwell International, Thousand Oaks, California 91360.

The Review of Scientific Instruments
|August 1, 1978
PubMed
Summary

A simple circuit maintains radio-frequency or microwave induced plasma continuity by monitoring reflected power. If plasma extinguishes, a high-voltage pulse is applied, ensuring stable plasma for various analytical techniques.

Area of Science:

  • Plasma Physics
  • Analytical Chemistry
  • Spectroscopy

Background:

  • Maintaining stable plasma is crucial for many analytical techniques.
  • Radio-frequency (RF) and microwave-induced plasmas are widely used in scientific applications.
  • Plasma extinction can disrupt experiments and lead to inaccurate results.

Purpose of the Study:

  • To describe a simple circuit for maintaining plasma continuity.
  • To enable stable operation of RF and microwave-induced plasmas.
  • To improve the reliability of plasma-based analytical methods.

Main Methods:

  • Monitoring reflected microwave power from the plasma discharge.
  • Detecting an increase in reflected power, indicating plasma extinction.
  • Applying a high-voltage pulse to a coil around the discharge region to re-ignite the plasma.

More Related Videos

Non-equilibrium Microwave Plasma for Efficient High Temperature Chemistry
07:17

Non-equilibrium Microwave Plasma for Efficient High Temperature Chemistry

Published on: August 1, 2017

An Atmospheric Pressure Plasma Setup to Investigate the Reactive Species Formation
08:36

An Atmospheric Pressure Plasma Setup to Investigate the Reactive Species Formation

Published on: November 3, 2016

Related Experiment Videos

Last Updated: Jul 2, 2026

How to Ignite an Atmospheric Pressure Microwave Plasma Torch without Any Additional Igniters
08:42

How to Ignite an Atmospheric Pressure Microwave Plasma Torch without Any Additional Igniters

Published on: April 16, 2015

Non-equilibrium Microwave Plasma for Efficient High Temperature Chemistry
07:17

Non-equilibrium Microwave Plasma for Efficient High Temperature Chemistry

Published on: August 1, 2017

An Atmospheric Pressure Plasma Setup to Investigate the Reactive Species Formation
08:36

An Atmospheric Pressure Plasma Setup to Investigate the Reactive Species Formation

Published on: November 3, 2016

Main Results:

  • The circuit effectively maintains plasma continuity.
  • Adjustable parameters include pulse repetition rate, voltage, and reflected power threshold.
  • Demonstrated applicability to resonance fluorescence, atomic absorption/emission, and kinetic determinations.

Conclusions:

  • The described circuit provides a simple and effective solution for plasma stabilization.
  • This technology enhances the reliability of plasma-dependent analytical measurements.
  • The circuit's versatility makes it suitable for diverse spectroscopic and kinetic analyses.