Related Experiment Video
Updated: Jul 2, 2026

MRM Microcoil Performance Calibration and Usage Demonstrated on Medicago truncatula Roots at 22 T
Published on: January 16, 2021
A convenient standard for low-field susceptibility calibration
J Rosenbaum1, E Larson, R Hoblitt
1Department of Geological Sciences, University of Colorado, Boulder, Colorado 80309, USA.
Calibration standards using magnetic iron oxide and glass powders offer moderate accuracy for low-field magnetic susceptibility measurements. These versatile powder mixtures are nearly linear with iron oxide concentration.
Area of Science:
- Geophysics and Materials Science
Background:
- Accurate magnetic susceptibility measurements are crucial in various scientific fields.
- Existing calibration standards may have limitations in terms of accuracy, shape, or size.
- Development of convenient and adaptable calibration standards is needed.
Purpose of the Study:
- To develop and characterize a novel calibration standard for low-field magnetic susceptibility measurements.
- To assess the accuracy and linearity of the proposed standard.
Main Methods:
- Preparation of finely ground mixtures of magnetic iron oxide and glass.
- Fabrication of calibration standards in various shapes and sizes using powder mixtures.
- Measurement of magnetic susceptibility for mixtures with varying iron oxide concentrations (0.063% to 11.8% by weight).
Main Results:
- The magnetic iron oxide-glass mixtures provide a calibration standard with moderate accuracy (approx. 5%).
- Susceptibility values ranged from 2.65 x 10(-7) to 5.77 x 10(-5) m3/kg.
- A nearly linear relationship was observed between magnetic susceptibility and iron oxide concentration.
Conclusions:
- Finely ground magnetic iron oxide and glass mixtures are effective calibration standards for low-field magnetic susceptibility.
- The powder form allows for versatile fabrication of standards.
- The linear response simplifies calibration and data interpretation.
Related Concept Videos
Calibration Curves: Linear Least Squares
For data that follow a straight line, the standard method for fitting is the linear...
Chemical Shift: Internal References and Solvent Effects
The internal reference compound generally used in NMR spectroscopy is tetramethylsilane (TMS). TMS is preferred because it is chemically inert, soluble in NMR solvents, and easily removable. Also, the highly shielded methyl protons in TMS yield an intense...
Magnetic Susceptibility and Permeability
When diamagnetic materials are placed under an external magnetic field, the moments opposite to the field are induced. Hence, the susceptibility for diamagnets has a minimal negative value of 10-5–10-6. Since...
Difference from Background: Limit of Detection
The LOD indicates the presence or absence...
Atomic Absorption Spectroscopy: Lab
Solutions containing organic solvents, such as low-molecular-mass alcohols, esters, or ketones, enhance absorbances by increasing nebulizer...

