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Synthesis and Microdiffraction at Extreme Pressures and Temperatures
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Versatile type miniature diamond anvil high-pressure cell.

S Yamaoka1, O Fukunaga, O Shimomura

  • 1National Institute for Researches in Inorganic Materials, Sakura-mura, Niihari-gun, Ibaraki 300-3l, Japan.

The Review of Scientific Instruments
|September 1, 1979
PubMed
Summary

Researchers developed a compact diamond anvil high-pressure cell capable of reaching 200 kbar. This versatile apparatus allows for easy and steady pressure generation, ideal for various high-pressure research applications.

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Area of Science:

  • Materials Science
  • Condensed Matter Physics
  • High-Pressure Science

Background:

  • High-pressure research requires specialized equipment for generating extreme pressures.
  • Existing high-pressure cells can be bulky, complex, or difficult to operate.
  • Miniaturization and improved accessibility are key for broader adoption of high-pressure techniques.

Purpose of the Study:

  • To construct a miniature diamond anvil high-pressure cell.
  • To achieve high and steady pressures with a compact and user-friendly device.
  • To enable versatile applications in high-pressure research.

Main Methods:

  • Construction of a miniature diamond anvil cell (42 mm diameter, 18 mm thick, 150 g).
  • Integration with a piston-cylinder pressing device featuring an alignment mechanism.
  • Pressure clamping using three screws for stable high-pressure generation.

Main Results:

  • Successfully constructed a small, lightweight, and simple high-pressure cell.
  • Achieved easy and steady pressure generation up to 200 kilobar (kbar).
  • The cell's design allows for mounting on a standard goniometer head with large access openings.

Conclusions:

  • The miniature diamond anvil cell offers a versatile and accessible apparatus for high-pressure research.
  • Its compact size and ease of use facilitate a wide range of experimental investigations.
  • This development simplifies and enhances the capability for conducting research at extreme pressures.