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Extractive spectrophotometric determination of TRODAT-1 hydrochloride in lyophilized kit

X M Li1, Z P Chen, S P Wang

  • 1Key Laboratory of Nuclear Medicine, Ministry of Health, Jiangsu Institute of Nuclear Medicine, Wuxi, Jiangsu, P.R. China.

Die Pharmazie
|September 30, 2008
PubMed

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Precipitation Titration: Endpoint Detection Methods01:19

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In argentometric precipitation titrations, endpoints can be detected visually by the Mohr, Volhard, and Fajans methods. In the Mohr method, adding a soluble chromate indicator gives an initial yellow color to the analyte solution. As the titrant is added, the first excess of silver ions forms a red silver chromate precipitate, marking the endpoint. The solution pH should be maintained at about 8 by adding solid CaCO3.
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