Precise and accurate quantitative (13)C NMR with reduced experimental time.

Elsa Caytan1, Gérald S Remaud, Eve Tenailleau

  • 1Nantes University, LAIEM-UMR-CNRS 6006, Faculty of Science and Technology, 2 rue de la Houssinière, BP 92208, F-44322 Nantes Cedex 3, France.

Talanta
|December 17, 2008
PubMed
Summary

High-sensitivity (13)C NMR requires precise measurements. Using (13)C bi-labelled ethanol as a probe, researchers found that reduced repetition delay with relaxation reagents maintains spectral quality for accurate isotopomer analysis.

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