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Related Experiment Video

Updated: Jun 27, 2026

Photodynamic Therapy with Blended Conducting Polymer/Fullerene Nanoparticle Photosensitizers
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Published on: October 28, 2015

Surgery of fullerenes.

Michihisa Murata1, Yasujiro Murata, Koichi Komatsu

  • 1Institute for Chemical Research, Kyoto University, Uji, Kyoto 611-0011, Japan.

Chemical Communications (Cambridge, England)
|December 17, 2008
PubMed
Summary
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Researchers synthesized endohedral fullerenes using molecular surgery. They created H(2)@C(60) and used the encapsulated hydrogen molecule as an NMR probe for ionic fullerene studies.

Area of Science:

  • Supramolecular Chemistry
  • Nanotechnology
  • Organic Chemistry

Background:

  • Endohedral fullerenes encapsulate atoms or molecules within fullerene cages.
  • Traditional synthesis methods are limited.
  • Molecular surgery offers a novel approach to endohedral fullerene synthesis.

Purpose of the Study:

  • To survey recent advances in endohedral fullerene synthesis via molecular surgery.
  • To detail the synthesis and properties of hydrogen molecule encapsulated in C(60) (H(2)@C(60)).
  • To explore the application of H(2)@C(60) as an NMR probe.

Main Methods:

  • Opening fullerene cages using organic reactions.
  • Encapsulating small molecules (He, H(2), H(2)O, CO) within the cages.
  • Developing effective methods for sealing the fullerene cage ('suturing').

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Last Updated: Jun 27, 2026

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  • Characterizing the synthesized endohedral fullerene H(2)@C(60).

    • Main Results:

    • Successful synthesis of H(2)@C(60) via molecular surgery.
    • Established effective 'suturing' techniques for fullerene cages.
    • Demonstrated the utility of encapsulated H(2) as an NMR probe.
    • Studied the properties and reactivity of H(2)@C(60).

    Conclusions:

    • Molecular surgery is a viable strategy for endohedral fullerene synthesis.
    • H(2)@C(60) is a novel endohedral fullerene with potential applications.
    • Encapsulated H(2) serves as a valuable NMR probe for studying ionic fullerenes.