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Microwave-assisted synthesis of N-substituted cyclic imides and their evaluation for anticancer and anti-inflammatory

Sham M Sondhi1, Reshma Rani, Partha Roy

  • 1Department of Chemistry, Indian Institute of Technology-Roorkee, Roorkee, Uttaranchal 247667, India.

Bioorganic & Medicinal Chemistry Letters
|February 10, 2009
PubMed

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Preparation of Amides01:29

Preparation of Amides

Amides are synthesized by treating carboxylic acids with amines in the presence of dehydrating agents like dicyclohexylcarbodiimide (DCC).
The DCC-promoted synthesis of amides begins with the protonation of DCC by carboxylic acid. The protonation makes it a better acceptor. Next, the addition of carboxylate to the protonated carbodiimide gives a reactive acylating agent.
Subsequently, the amine acts as a nucleophile that attacks the acylating agent to form a tetrahedral intermediate. In the...