Search research articles

ABOUT JoVE

Overview Leadership Blog JoVE Help Center

AUTHORS

Publishing Process Editorial Board Scope & Policies Peer Review FAQ Submit

LIBRARIANS

Testimonials Subscriptions Access Resources Library Advisory Board FAQ

RESEARCH

JoVE Journal Methods Collections JoVE Encyclopedia of Experiments Archive

EDUCATION

JoVE Core JoVE Business JoVE Science Education JoVE Lab Manual Faculty Resource Center Faculty Site

Terms & Conditions of Use

Related Concept Videos

$X-ray Diffraction of Biological Samples$ 01:10

X-ray Diffraction of Biological Samples

X-ray diffraction or XRD is an analytical tool that utilizes X-rays to study ordered structures such as crystalline organic and inorganic samples, polycrystalline materials, proteins, carbohydrates, and drugs.
According to Bragg's law, when X-rays strike the sample positioned on a stage, the rays are scattered by the electron clouds around the sample atoms. The X-ray diffraction or scattering is caused by constructive interference of the X-ray waves that reflect off the internal crystal...

You might also read

Related Articles

Articles linked to this work by shared authors, journal, and citation graph.

Sort by

Same author

Momentum-Resolved X-Ray Thomson Scattering Benchmark of Electronic-Response Models in Warm Dense Aluminium.

Physical review letters·2026

Same author

Adaptive filtering method for reducing signal saturation induced artifacts in X-ray dark-field tomography.

Scientific reports·2026

Same author

Dynamics of coalescence in hyperquenched glassy water probed by x-rays.

The Journal of chemical physics·2026

Same author

A pipeline for megahertz X-ray photon correlation spectroscopy on soft matter samples at the MID instrument of European XFEL.

Journal of synchrotron radiation·2026

Same author

Unveiling Zn Incorporation in CuInS<sub>2</sub> Quantum Dots: X‑ray and Optical Analysis of Doping Effects, Structural Modifications, and Surface Passivation.

Chemistry of materials : a publication of the American Chemical Society·2026

Same author

Influence of redox atmospheres on selenate retention by mackinawite, magnetite and pyrite.

Journal of hazardous materials·2026

Search research articles

Related Experiment Video

Updated: Jun 25, 2026

Hyperpolarized Xenon for NMR and MRI Applications

Hyperpolarized Xenon for NMR and MRI Applications

Published on: September 6, 2012

A sample cell to study hydrate formation with x-ray scattering.

Heiko Conrad¹, Felix Lehmkühler, Christian Sternemann

¹Fakultät Physik/DELTA, Technische Universität Dortmund, Maria-Goeppert-Mayer-Str. 2,Dortmund D-44221, Germany. heiko.conrad@tu-dortmund.de

The Review of Scientific Instruments

|March 5, 2009

Summary

This summary is machine-generated.

Researchers developed a novel sample cell for inelastic X-ray scattering. This new cell enables in situ formation and study of tetrahydrofuran (THF) hydrates and liquid mixtures, advancing hydrate research.

More Related Videos

Experimental Study of the Relationship Between Particle Size and Methane Sorption Capacity in Shale

Experimental Study of the Relationship Between Particle Size and Methane Sorption Capacity in Shale

Published on: August 2, 2018

Fabrication of a Dipole-assisted Solid Phase Extraction Microchip for Trace Metal Analysis in Water Samples

Fabrication of a Dipole-assisted Solid Phase Extraction Microchip for Trace Metal Analysis in Water Samples

Published on: August 7, 2016

Related Experiment Videos

Last Updated: Jun 25, 2026

Hyperpolarized Xenon for NMR and MRI Applications

Hyperpolarized Xenon for NMR and MRI Applications

Published on: September 6, 2012

Experimental Study of the Relationship Between Particle Size and Methane Sorption Capacity in Shale

Experimental Study of the Relationship Between Particle Size and Methane Sorption Capacity in Shale

Published on: August 2, 2018

Fabrication of a Dipole-assisted Solid Phase Extraction Microchip for Trace Metal Analysis in Water Samples

Fabrication of a Dipole-assisted Solid Phase Extraction Microchip for Trace Metal Analysis in Water Samples

Published on: August 7, 2016

Area of Science:

Materials Science
Chemistry
Physics

Background:

Studying liquid mixtures and hydrates requires specialized sample environments.
In situ sample preparation and characterization are crucial for understanding dynamic processes.

Purpose of the Study:

To present a new sample cell designed for in situ nonresonant inelastic X-ray scattering (NIXS) measurements.
To demonstrate the cell's capability in forming and analyzing tetrahydrofuran (THF) hydrates and THF-water mixtures.

Main Methods:

Utilized a novel sample cell with a magnetic stirring mechanism for hydrate nucleation.
Employed wide-angle X-ray scattering (WAXS) and oxygen K-edge nonresonant X-ray Raman scattering (XRS) for hydrate verification.
Performed nonresonant inelastic X-ray scattering (NIXS) across a broad range of scattering angles.

Main Results:

Successfully formed tetrahydrofuran (THF) hydrates within the sample cell.
Verified hydrate formation using WAXS and oxygen K-edge NIXS.
Demonstrated the cell's suitability for momentum transfer-dependent NIXS studies.

Conclusions:

The developed sample cell is effective for in situ formation and characterization of liquid mixtures and hydrates.
This versatile cell can be applied to study other liquid hydrate formers and in situ mixed liquid samples.
The cell facilitates detailed investigation of materials using momentum transfer-dependent NIXS.